TY - JOUR
T1 - Comparison of synthesis methods of Tb MOF
T2 - 11th International Congress of Physics Engineering, CIIF 2021
AU - Sánchez-Moreno, Diana L.
AU - Loera-Serna, Sandra
AU - Garduño-Wilches, Ismael A.
AU - Aguilar Frutis, Miguel A.
AU - Alarcón-Flores, Gilberto
N1 - Publisher Copyright:
© 2022 Published under licence by IOP Publishing Ltd.
PY - 2022
Y1 - 2022
N2 - This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.
AB - This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.
UR - http://www.scopus.com/inward/record.url?scp=85141884300&partnerID=8YFLogxK
U2 - 10.1088/1742-6596/2307/1/012057
DO - 10.1088/1742-6596/2307/1/012057
M3 - Artículo de la conferencia
AN - SCOPUS:85141884300
SN - 1742-6588
VL - 2307
JO - Journal of Physics: Conference Series
JF - Journal of Physics: Conference Series
IS - 1
M1 - 012057
Y2 - 26 September 2021 through 29 September 2021
ER -