Comparison of synthesis methods of Tb MOF: microwave and metathesis

Diana L. Sánchez-Moreno; Sandra Loera-Serna; Ismael A. Garduño-Wilches; Miguel A. Aguilar Frutis; Gilberto Alarcón-Flores

doi:10.1088/1742-6596/2307/1/012057

Comparison of synthesis methods of Tb MOF: microwave and metathesis

Diana L. Sánchez-Moreno, Sandra Loera-Serna, Ismael A. Garduño-Wilches, Miguel A. Aguilar Frutis, Gilberto Alarcón-Flores

Research output: Contribution to journal › Conference article › peer-review

Abstract

This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.

Original language	English
Article number	012057
Journal	Journal of Physics: Conference Series
Volume	2307
Issue number	1
DOIs	https://doi.org/10.1088/1742-6596/2307/1/012057
State	Published - 2022
Externally published	Yes
Event	11th International Congress of Physics Engineering, CIIF 2021 - Mexico City, Mexico Duration: 26 Sep 2021 → 29 Sep 2021

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title = "Comparison of synthesis methods of Tb MOF: microwave and metathesis",

abstract = "This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.",

author = "S{\'a}nchez-Moreno, {Diana L.} and Sandra Loera-Serna and Gardu{\~n}o-Wilches, {Ismael A.} and {Aguilar Frutis}, {Miguel A.} and Gilberto Alarc{\'o}n-Flores",

note = "Publisher Copyright: {\textcopyright} 2022 Published under licence by IOP Publishing Ltd.; 11th International Congress of Physics Engineering, CIIF 2021 ; Conference date: 26-09-2021 Through 29-09-2021",

year = "2022",

doi = "10.1088/1742-6596/2307/1/012057",

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TY - JOUR

T1 - Comparison of synthesis methods of Tb MOF

T2 - 11th International Congress of Physics Engineering, CIIF 2021

AU - Sánchez-Moreno, Diana L.

AU - Loera-Serna, Sandra

AU - Garduño-Wilches, Ismael A.

AU - Aguilar Frutis, Miguel A.

AU - Alarcón-Flores, Gilberto

PY - 2022

Y1 - 2022

N2 - This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.

AB - This paper presents the synthesis of the metal-organic structure of terbium Tb2(BDC)3 (BDC: 1,4-benzendicarboxylic acid) obtained by stirring at room temperature (SRT) and by means of the microwave-assisted synthesis method (MW) at 150 °C during 15 min. A comparison was made between the physicochemical properties of the MOF obtained by each of the methods as they were characterized by powder X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR), observing crystalline materials with crystal size 66.42 and 26.57 nm for SRT and MW, respectively. The luminescent properties were determined by photoluminescent spectroscopy (FL) and finally the morphology presented by MW synthesis.

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U2 - 10.1088/1742-6596/2307/1/012057

DO - 10.1088/1742-6596/2307/1/012057

M3 - Artículo de la conferencia

AN - SCOPUS:85141884300

SN - 1742-6588

VL - 2307

JO - Journal of Physics: Conference Series

JF - Journal of Physics: Conference Series

IS - 1

M1 - 012057

Y2 - 26 September 2021 through 29 September 2021

ER -

Comparison of synthesis methods of Tb MOF: microwave and metathesis

Abstract

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