Pushing the limits of signal resolution to make coupling measurement easier

José Enrique Herbert Pucheta; Daisy Pitoux; Claire M. Grison; Sylvie Robin; Denis Merlet; David J. Aitken; Nicolas Giraud; Jonathan Farjon

doi:10.1039/c5cc01305d

Pushing the limits of signal resolution to make coupling measurement easier

José Enrique Herbert Pucheta, Daisy Pitoux, Claire M. Grison, Sylvie Robin, Denis Merlet, David J. Aitken, Nicolas Giraud, Jonathan Farjon

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

26 Citas (Scopus)

Resumen

Probing scalar couplings are essential for structural elucidation in molecular (bio)chemistry. While the measurement of J_HH couplings is facilitated by SERF experiments, overcrowded signals represent a significant limitation. Here, a new band selective pure shift SERF allows access to δ¹H and J_HH with an ultrahigh spectral resolution.

Idioma original	Inglés
Páginas (desde-hasta)	7939-7942
Número de páginas	4
Publicación	Chemical Communications
Volumen	51
N.º	37
DOI	https://doi.org/10.1039/c5cc01305d
Estado	Publicada - 7 may. 2015
Publicado de forma externa	Sí

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abstract = "Probing scalar couplings are essential for structural elucidation in molecular (bio)chemistry. While the measurement of JHH couplings is facilitated by SERF experiments, overcrowded signals represent a significant limitation. Here, a new band selective pure shift SERF allows access to δ1H and JHH with an ultrahigh spectral resolution.",

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AU - Herbert Pucheta, José Enrique

AU - Pitoux, Daisy

AU - Grison, Claire M.

AU - Robin, Sylvie

AU - Merlet, Denis

AU - Aitken, David J.

AU - Giraud, Nicolas

AU - Farjon, Jonathan

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AB - Probing scalar couplings are essential for structural elucidation in molecular (bio)chemistry. While the measurement of JHH couplings is facilitated by SERF experiments, overcrowded signals represent a significant limitation. Here, a new band selective pure shift SERF allows access to δ1H and JHH with an ultrahigh spectral resolution.

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Pushing the limits of signal resolution to make coupling measurement easier

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