Characterization of Mercury Jarosite

Sayra Ordoñez; Francisco Patiño; Mizraim Uriel Flores; Iván Alejandro Reyes; Elia Guadalupe Palacios; Víctor Hugo Flores; Martín Reyes; Ister Mireles; Hernán Islas

doi:10.1007/978-3-319-51382-9_64

Characterization of Mercury Jarosite

Sayra Ordoñez, Francisco Patiño, Mizraim Uriel Flores, Iván Alejandro Reyes, Elia Guadalupe Palacios, Víctor Hugo Flores, Martín Reyes, Ister Mireles, Hernán Islas

Producción científica: Capítulo del libro/informe/acta de congreso › Contribución a la conferencia › revisión exhaustiva

1 Cita (Scopus)

Resumen

This paper presents the characterization of a sample of mercury jarosite that was synthesized by slowly adding Hg(NO₃)₂·H₂O into a Fe₂(SO₄)₃·nH₂O solution. X-ray diffraction (XRD) analysis performed on the sample confirmed that the compound presents a crystal phase corresponding to mercury jarosite. Analysis through Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM-EDS) determined that the precipitate is composed of mercury, sulfur, iron and oxygen. It is made up of spherical particles with an average size of 38µm; these particles are made of rhombohedral micro-crystals with sizes ranging between 1 and 2µm. Chemical characterization was performed through dichromatometry analysis, gravimetry and atomic absorption spectroscopy (AAS), thus obtaining the following composition: 27% Fe³⁺, 37% SO₄ ²⁻ 14% Hg²⁺, 22% OH⁻+H₃O⁺+H₂O. The following approximate formula of the compound was determined from chemical analysis: [Hg_0.39(H₃O)_0.22]Fe_2.71(SO₄)_2.17(OH)_4.79(H₂O)_2.09.

Idioma original	Inglés
Título de la publicación alojada	Characterization of Minerals, Metals, and Materials 2017
Editores	Jian Li, Sergio Neves Monteiro, Juan P. Escobedo-Diaz, Jeongguk Kim, Ramasis Goswami, Jiann-Yang Hwang, Yunus Eren Kalay, Bowen Li, Mingming Zhang, Shadia Ikhmayies, John S. Carpenter, Zhiwei Peng, Donato Firrao, Chenguang Bai
Editorial	Springer International Publishing
Páginas	585-592
Número de páginas	8
ISBN (versión impresa)	9783319513812
DOI	https://doi.org/10.1007/978-3-319-51382-9_64
Estado	Publicada - 2017
Publicado de forma externa	Sí
Evento	International Symposium on Characterization of Minerals, Metals, and Materials, 2017 - San Diego, Estados Unidos Duración: 26 feb. 2017 → 2 mar. 2017

Serie de la publicación

Nombre	Minerals, Metals and Materials Series
Volumen	Part F7
ISSN (versión impresa)	2367-1181
ISSN (versión digital)	2367-1696

Conferencia

Conferencia	International Symposium on Characterization of Minerals, Metals, and Materials, 2017
País/Territorio	Estados Unidos
Ciudad	San Diego
Período	26/02/17 → 2/03/17

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10.1007/978-3-319-51382-9_64

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Ordoñez, S., Patiño, F., Flores, M. U., Reyes, I. A., Palacios, E. G., Flores, V. H., Reyes, M., Mireles, I., & Islas, H. (2017). Characterization of Mercury Jarosite. En J. Li, S. N. Monteiro, J. P. Escobedo-Diaz, J. Kim, R. Goswami, J.-Y. Hwang, Y. E. Kalay, B. Li, M. Zhang, S. Ikhmayies, J. S. Carpenter, Z. Peng, D. Firrao, & C. Bai (Eds.), Characterization of Minerals, Metals, and Materials 2017 (pp. 585-592). (Minerals, Metals and Materials Series; Vol. Part F7). Springer International Publishing. https://doi.org/10.1007/978-3-319-51382-9_64

Ordoñez, Sayra ; Patiño, Francisco ; Flores, Mizraim Uriel et al. / Characterization of Mercury Jarosite. Characterization of Minerals, Metals, and Materials 2017. editor / Jian Li ; Sergio Neves Monteiro ; Juan P. Escobedo-Diaz ; Jeongguk Kim ; Ramasis Goswami ; Jiann-Yang Hwang ; Yunus Eren Kalay ; Bowen Li ; Mingming Zhang ; Shadia Ikhmayies ; John S. Carpenter ; Zhiwei Peng ; Donato Firrao ; Chenguang Bai. Springer International Publishing, 2017. pp. 585-592 (Minerals, Metals and Materials Series).

@inproceedings{93f3e4edff89435482f98b104ec1442a,

title = "Characterization of Mercury Jarosite",

abstract = "This paper presents the characterization of a sample of mercury jarosite that was synthesized by slowly adding Hg(NO3)2·H2O into a Fe2(SO4)3·nH2O solution. X-ray diffraction (XRD) analysis performed on the sample confirmed that the compound presents a crystal phase corresponding to mercury jarosite. Analysis through Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM-EDS) determined that the precipitate is composed of mercury, sulfur, iron and oxygen. It is made up of spherical particles with an average size of 38µm; these particles are made of rhombohedral micro-crystals with sizes ranging between 1 and 2µm. Chemical characterization was performed through dichromatometry analysis, gravimetry and atomic absorption spectroscopy (AAS), thus obtaining the following composition: 27% Fe3+, 37% SO4 2− 14% Hg2+, 22% OH−+H3O++H2O. The following approximate formula of the compound was determined from chemical analysis: [Hg0.39(H3O)0.22]Fe2.71(SO4)2.17(OH)4.79(H2O)2.09.",

keywords = "Characterization, Jarosite, Mercury",

author = "Sayra Ordo{\~n}ez and Francisco Pati{\~n}o and Flores, {Mizraim Uriel} and Reyes, {Iv{\'a}n Alejandro} and Palacios, {Elia Guadalupe} and Flores, {V{\'i}ctor Hugo} and Mart{\'i}n Reyes and Ister Mireles and Hern{\'a}n Islas",

note = "Publisher Copyright: {\textcopyright} The Minerals, Metals & Materials Society 2017.; International Symposium on Characterization of Minerals, Metals, and Materials, 2017 ; Conference date: 26-02-2017 Through 02-03-2017",

year = "2017",

doi = "10.1007/978-3-319-51382-9_64",

language = "Ingl{\'e}s",

isbn = "9783319513812",

series = "Minerals, Metals and Materials Series",

publisher = "Springer International Publishing",

pages = "585--592",

editor = "Jian Li and Monteiro, {Sergio Neves} and Escobedo-Diaz, {Juan P.} and Jeongguk Kim and Ramasis Goswami and Jiann-Yang Hwang and Kalay, {Yunus Eren} and Bowen Li and Mingming Zhang and Shadia Ikhmayies and Carpenter, {John S.} and Zhiwei Peng and Donato Firrao and Chenguang Bai",

booktitle = "Characterization of Minerals, Metals, and Materials 2017",

}

Ordoñez, S, Patiño, F, Flores, MU, Reyes, IA, Palacios, EG, Flores, VH, Reyes, M, Mireles, I & Islas, H 2017, Characterization of Mercury Jarosite. En J Li, SN Monteiro, JP Escobedo-Diaz, J Kim, R Goswami, J-Y Hwang, YE Kalay, B Li, M Zhang, S Ikhmayies, JS Carpenter, Z Peng, D Firrao & C Bai (eds.), Characterization of Minerals, Metals, and Materials 2017. Minerals, Metals and Materials Series, vol. Part F7, Springer International Publishing, pp. 585-592, International Symposium on Characterization of Minerals, Metals, and Materials, 2017, San Diego, Estados Unidos, 26/02/17. https://doi.org/10.1007/978-3-319-51382-9_64

Characterization of Mercury Jarosite. / Ordoñez, Sayra; Patiño, Francisco; Flores, Mizraim Uriel et al.
Characterization of Minerals, Metals, and Materials 2017. ed. / Jian Li; Sergio Neves Monteiro; Juan P. Escobedo-Diaz; Jeongguk Kim; Ramasis Goswami; Jiann-Yang Hwang; Yunus Eren Kalay; Bowen Li; Mingming Zhang; Shadia Ikhmayies; John S. Carpenter; Zhiwei Peng; Donato Firrao; Chenguang Bai. Springer International Publishing, 2017. p. 585-592 (Minerals, Metals and Materials Series; Vol. Part F7).

Producción científica: Capítulo del libro/informe/acta de congreso › Contribución a la conferencia › revisión exhaustiva

TY - GEN

T1 - Characterization of Mercury Jarosite

AU - Ordoñez, Sayra

AU - Patiño, Francisco

AU - Flores, Mizraim Uriel

AU - Reyes, Iván Alejandro

AU - Palacios, Elia Guadalupe

AU - Flores, Víctor Hugo

AU - Reyes, Martín

AU - Mireles, Ister

AU - Islas, Hernán

N1 - Publisher Copyright: © The Minerals, Metals & Materials Society 2017.

PY - 2017

Y1 - 2017

N2 - This paper presents the characterization of a sample of mercury jarosite that was synthesized by slowly adding Hg(NO3)2·H2O into a Fe2(SO4)3·nH2O solution. X-ray diffraction (XRD) analysis performed on the sample confirmed that the compound presents a crystal phase corresponding to mercury jarosite. Analysis through Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM-EDS) determined that the precipitate is composed of mercury, sulfur, iron and oxygen. It is made up of spherical particles with an average size of 38µm; these particles are made of rhombohedral micro-crystals with sizes ranging between 1 and 2µm. Chemical characterization was performed through dichromatometry analysis, gravimetry and atomic absorption spectroscopy (AAS), thus obtaining the following composition: 27% Fe3+, 37% SO4 2− 14% Hg2+, 22% OH−+H3O++H2O. The following approximate formula of the compound was determined from chemical analysis: [Hg0.39(H3O)0.22]Fe2.71(SO4)2.17(OH)4.79(H2O)2.09.

AB - This paper presents the characterization of a sample of mercury jarosite that was synthesized by slowly adding Hg(NO3)2·H2O into a Fe2(SO4)3·nH2O solution. X-ray diffraction (XRD) analysis performed on the sample confirmed that the compound presents a crystal phase corresponding to mercury jarosite. Analysis through Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM-EDS) determined that the precipitate is composed of mercury, sulfur, iron and oxygen. It is made up of spherical particles with an average size of 38µm; these particles are made of rhombohedral micro-crystals with sizes ranging between 1 and 2µm. Chemical characterization was performed through dichromatometry analysis, gravimetry and atomic absorption spectroscopy (AAS), thus obtaining the following composition: 27% Fe3+, 37% SO4 2− 14% Hg2+, 22% OH−+H3O++H2O. The following approximate formula of the compound was determined from chemical analysis: [Hg0.39(H3O)0.22]Fe2.71(SO4)2.17(OH)4.79(H2O)2.09.

KW - Characterization

KW - Jarosite

KW - Mercury

UR - http://www.scopus.com/inward/record.url?scp=85033699980&partnerID=8YFLogxK

U2 - 10.1007/978-3-319-51382-9_64

DO - 10.1007/978-3-319-51382-9_64

M3 - Contribución a la conferencia

SN - 9783319513812

T3 - Minerals, Metals and Materials Series

SP - 585

EP - 592

BT - Characterization of Minerals, Metals, and Materials 2017

A2 - Li, Jian

A2 - Monteiro, Sergio Neves

A2 - Escobedo-Diaz, Juan P.

A2 - Kim, Jeongguk

A2 - Goswami, Ramasis

A2 - Hwang, Jiann-Yang

A2 - Kalay, Yunus Eren

A2 - Li, Bowen

A2 - Zhang, Mingming

A2 - Ikhmayies, Shadia

A2 - Carpenter, John S.

A2 - Peng, Zhiwei

A2 - Firrao, Donato

A2 - Bai, Chenguang

PB - Springer International Publishing

T2 - International Symposium on Characterization of Minerals, Metals, and Materials, 2017

Y2 - 26 February 2017 through 2 March 2017

ER -

Ordoñez S, Patiño F, Flores MU, Reyes IA, Palacios EG, Flores VH et al. Characterization of Mercury Jarosite. En Li J, Monteiro SN, Escobedo-Diaz JP, Kim J, Goswami R, Hwang JY, Kalay YE, Li B, Zhang M, Ikhmayies S, Carpenter JS, Peng Z, Firrao D, Bai C, editores, Characterization of Minerals, Metals, and Materials 2017. Springer International Publishing. 2017. p. 585-592. (Minerals, Metals and Materials Series). doi: 10.1007/978-3-319-51382-9_64

Characterization of Mercury Jarosite

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