Synthesis of molybdenum oxide microsheets via close-spaced vapor transport

O. Goiz, F. Chávez, C. Felipe, N. Morales, R. Peña-Sierra

Research output: Contribution to conferencePaper

4 Citations (Scopus)

Abstract

Growth of molybdenum oxide microsheets on silicon (1 0 0) substrates using the close-spaced vapor transport (CSVT) technique is proposed. Molybdenum oxide powder is employed as source, the synthesis is carried out at atmospheric pressure with a nitrogen ambient by employing short times (a few minutes), water as reactant and moderate temperatures. The growth process is efficient, fast, and without the use of catalysts. Changes in morphology and structure of products when temperature varies are reported. The produced molybdenum oxide microsheets are analyzed with SEM, XRD and micro-Raman techniques. © 2010 Elsevier B.V. All rights reserved.
Original languageAmerican English
Pages174-176
Number of pages156
DOIs
StatePublished - 25 Oct 2010
EventMaterials Science and Engineering B: Solid-State Materials for Advanced Technology -
Duration: 25 Oct 2010 → …

Conference

ConferenceMaterials Science and Engineering B: Solid-State Materials for Advanced Technology
Period25/10/10 → …

Fingerprint

Molybdenum oxide
molybdenum
Vapors
oxide
atmospheric pressure
silicon
Atmospheric pressure
temperature
catalyst
scanning electron microscopy
X-ray diffraction
Nitrogen
Powders
substrate
Silicon
Temperature
Scanning electron microscopy
Catalysts
nitrogen
Substrates

Cite this

Goiz, O., Chávez, F., Felipe, C., Morales, N., & Peña-Sierra, R. (2010). Synthesis of molybdenum oxide microsheets via close-spaced vapor transport. 174-176. Paper presented at Materials Science and Engineering B: Solid-State Materials for Advanced Technology, . https://doi.org/10.1016/j.mseb.2010.03.021
Goiz, O. ; Chávez, F. ; Felipe, C. ; Morales, N. ; Peña-Sierra, R. / Synthesis of molybdenum oxide microsheets via close-spaced vapor transport. Paper presented at Materials Science and Engineering B: Solid-State Materials for Advanced Technology, .156 p.
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Goiz, O, Chávez, F, Felipe, C, Morales, N & Peña-Sierra, R 2010, 'Synthesis of molybdenum oxide microsheets via close-spaced vapor transport', Paper presented at Materials Science and Engineering B: Solid-State Materials for Advanced Technology, 25/10/10 pp. 174-176. https://doi.org/10.1016/j.mseb.2010.03.021

Synthesis of molybdenum oxide microsheets via close-spaced vapor transport. / Goiz, O.; Chávez, F.; Felipe, C.; Morales, N.; Peña-Sierra, R.

2010. 174-176 Paper presented at Materials Science and Engineering B: Solid-State Materials for Advanced Technology, .

Research output: Contribution to conferencePaper

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AB - Growth of molybdenum oxide microsheets on silicon (1 0 0) substrates using the close-spaced vapor transport (CSVT) technique is proposed. Molybdenum oxide powder is employed as source, the synthesis is carried out at atmospheric pressure with a nitrogen ambient by employing short times (a few minutes), water as reactant and moderate temperatures. The growth process is efficient, fast, and without the use of catalysts. Changes in morphology and structure of products when temperature varies are reported. The produced molybdenum oxide microsheets are analyzed with SEM, XRD and micro-Raman techniques. © 2010 Elsevier B.V. All rights reserved.

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Goiz O, Chávez F, Felipe C, Morales N, Peña-Sierra R. Synthesis of molybdenum oxide microsheets via close-spaced vapor transport. 2010. Paper presented at Materials Science and Engineering B: Solid-State Materials for Advanced Technology, . https://doi.org/10.1016/j.mseb.2010.03.021