TY - JOUR
T1 - Synthesis and characterization of nickel antimonate nanoparticles
T2 - sensing properties in propane and carbon monoxide
AU - Guillén-Bonilla, Héctor
AU - Olvera-Amador, M. de la Luz
AU - Casallas-Moreno, Y. L.
AU - Guillén-Bonilla, José Trinidad
AU - Guillén-Bonilla, Alex
AU - Gildo-Ortiz, Lorenzo
AU - Morán-Lázaro, Juan Pablo
AU - Santoyo-Salazar, Jaime
AU - Rodríguez-Betancourtt, Verónica M.
N1 - Publisher Copyright:
© 2019, Springer Science+Business Media, LLC, part of Springer Nature.
PY - 2019/3/1
Y1 - 2019/3/1
N2 - Nickel antimonate (NiSb 2 O 6 ) was synthesized by a microwave-assisted wet chemical method for its application as a potential gas sensor. The powders calcined at 600 °C were corroborated by X-ray diffraction. The microstructure of the material was analyzed by electron microscopy in its scanning and transmission versions, finding different morphologies. The average size of the nanoparticles was estimated at ~ 14.3 nm. X-ray photoelectron spectroscopy showed that the bond energies for Ni (2p) were of 855.2 and 872.9 eV, for Sb, they were of 530.28 and 539.66 eV, and for O(1s), it overlapped the Sb at 530.28 eV. Photoluminescence and UV–Vis spectroscopy measurements confirmed that the emission energy values were of 2.8 and 1.4 eV. Tests carried out in propane and CO atmospheres indicated that the NiSb 2 O 6 nanoparticles possess good response at several concentrations and temperatures of both gases. According to our results, NiSb 2 O 6 is a strong candidate to be applied as a gas sensor.
AB - Nickel antimonate (NiSb 2 O 6 ) was synthesized by a microwave-assisted wet chemical method for its application as a potential gas sensor. The powders calcined at 600 °C were corroborated by X-ray diffraction. The microstructure of the material was analyzed by electron microscopy in its scanning and transmission versions, finding different morphologies. The average size of the nanoparticles was estimated at ~ 14.3 nm. X-ray photoelectron spectroscopy showed that the bond energies for Ni (2p) were of 855.2 and 872.9 eV, for Sb, they were of 530.28 and 539.66 eV, and for O(1s), it overlapped the Sb at 530.28 eV. Photoluminescence and UV–Vis spectroscopy measurements confirmed that the emission energy values were of 2.8 and 1.4 eV. Tests carried out in propane and CO atmospheres indicated that the NiSb 2 O 6 nanoparticles possess good response at several concentrations and temperatures of both gases. According to our results, NiSb 2 O 6 is a strong candidate to be applied as a gas sensor.
UR - http://www.scopus.com/inward/record.url?scp=85061914453&partnerID=8YFLogxK
U2 - 10.1007/s10854-019-00918-9
DO - 10.1007/s10854-019-00918-9
M3 - Artículo
SN - 0957-4522
VL - 30
SP - 6166
EP - 6177
JO - Journal of Materials Science: Materials in Electronics
JF - Journal of Materials Science: Materials in Electronics
IS - 6
ER -