Structural Characterization of Europium-Doped BaTiO3 Obtained by Solid-State Reaction Synthesis

J. P. Hernández-Lara; A. Hernández-Ramírez; J. A. Romero-Serrano; M. Pérez-Labra; F. R. Barrientos-Hernández; R. Martinez-Lopez; M. I. Valenzuela-Carrillo

doi:10.1007/978-3-031-22576-5_56

Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis

J. P. Hernández-Lara, A. Hernández-Ramírez, J. A. Romero-Serrano, M. Pérez-Labra, F. R. Barrientos-Hernández, R. Martinez-Lopez, M. I. Valenzuela-Carrillo

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Barium Titanate (BaTiO₃)-based ceramic materials are widely used in the electroceramic industry. Conventional processing of these materials is primarily in high-temperature solid-state reactions between mixed oxides. To produce a better quality of the initial powder, factors such as the quality of raw materials, homogeneity of the mixture and the nature of the reaction atmosphere must be controlled. In this research, an analysis of BaTiO₃-based ceramic products doped with Europium (Eu³⁺) were carried out, by means of solid-state reaction synthesis. A review of the compositions (x = 0.007 and x = 0.01% by weight Eu³⁺) was carried out, grinding was carried out for 5 h and the resulting powders were calcined at 900 °C and sintered at 1350 °C. The experimental results by x-ray diffraction showed the tetragonal BaTiO₃ phase. Raman spectroscopy analysis shows the phase transition of BaTiO₃ ceramics. Scanning electron microscopy results showed randomly round particles.

Original language	English
Title of host publication	Characterization of Minerals, Metals, and Materials 2023
Editors	Mingming Zhang, Zhiwei Peng, Bowen Li, Jiann-Yang Hwang, Sergio Neves Monteiro, Rajiv Soman, Yunus Eren Kalay, Juan P. Escobedo-Diaz, John S. Carpenter, Andrew D. Brown, Shadia Ikhmayies
Publisher	Springer Science and Business Media Deutschland GmbH
Pages	553-559
Number of pages	7
ISBN (Print)	9783031225758
DOIs	https://doi.org/10.1007/978-3-031-22576-5_56
State	Published - 2023
Externally published	Yes
Event	Characterization of Minerals, Metals, and Materials Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023 - San Diego, United States Duration: 19 Mar 2023 → 23 Mar 2023

Publication series

Name	Minerals, Metals and Materials Series
ISSN (Print)	2367-1181
ISSN (Electronic)	2367-1696

Conference

Conference	Characterization of Minerals, Metals, and Materials Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023
Country/Territory	United States
City	San Diego
Period	19/03/23 → 23/03/23

Keywords

Europium
Raman spectroscopy
Solid state reaction

Access to Document

10.1007/978-3-031-22576-5_56

Cite this

Hernández-Lara, J. P., Hernández-Ramírez, A., Romero-Serrano, J. A., Pérez-Labra, M., Barrientos-Hernández, F. R., Martinez-Lopez, R., & Valenzuela-Carrillo, M. I. (2023). Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis. In M. Zhang, Z. Peng, B. Li, J.-Y. Hwang, S. N. Monteiro, R. Soman, Y. E. Kalay, J. P. Escobedo-Diaz, J. S. Carpenter, A. D. Brown, & S. Ikhmayies (Eds.), Characterization of Minerals, Metals, and Materials 2023 (pp. 553-559). (Minerals, Metals and Materials Series). Springer Science and Business Media Deutschland GmbH. https://doi.org/10.1007/978-3-031-22576-5_56

Hernández-Lara, J. P. ; Hernández-Ramírez, A. ; Romero-Serrano, J. A. et al. / Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis. Characterization of Minerals, Metals, and Materials 2023. editor / Mingming Zhang ; Zhiwei Peng ; Bowen Li ; Jiann-Yang Hwang ; Sergio Neves Monteiro ; Rajiv Soman ; Yunus Eren Kalay ; Juan P. Escobedo-Diaz ; John S. Carpenter ; Andrew D. Brown ; Shadia Ikhmayies. Springer Science and Business Media Deutschland GmbH, 2023. pp. 553-559 (Minerals, Metals and Materials Series).

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title = "Structural Characterization of Europium-Doped BaTiO3 Obtained by Solid-State Reaction Synthesis",

abstract = "Barium Titanate (BaTiO3)-based ceramic materials are widely used in the electroceramic industry. Conventional processing of these materials is primarily in high-temperature solid-state reactions between mixed oxides. To produce a better quality of the initial powder, factors such as the quality of raw materials, homogeneity of the mixture and the nature of the reaction atmosphere must be controlled. In this research, an analysis of BaTiO3-based ceramic products doped with Europium (Eu3+) were carried out, by means of solid-state reaction synthesis. A review of the compositions (x = 0.007 and x = 0.01% by weight Eu3+) was carried out, grinding was carried out for 5 h and the resulting powders were calcined at 900 °C and sintered at 1350 °C. The experimental results by x-ray diffraction showed the tetragonal BaTiO3 phase. Raman spectroscopy analysis shows the phase transition of BaTiO3 ceramics. Scanning electron microscopy results showed randomly round particles.",

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Hernández-Lara, JP, Hernández-Ramírez, A , Romero-Serrano, JA, Pérez-Labra, M, Barrientos-Hernández, FR, Martinez-Lopez, R & Valenzuela-Carrillo, MI 2023, Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis. in M Zhang, Z Peng, B Li, J-Y Hwang, SN Monteiro, R Soman, YE Kalay, JP Escobedo-Diaz, JS Carpenter, AD Brown & S Ikhmayies (eds), Characterization of Minerals, Metals, and Materials 2023. Minerals, Metals and Materials Series, Springer Science and Business Media Deutschland GmbH, pp. 553-559, Characterization of Minerals, Metals, and Materials Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023, San Diego, United States, 19/03/23. https://doi.org/10.1007/978-3-031-22576-5_56

Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis. / Hernández-Lara, J. P.; Hernández-Ramírez, A.; Romero-Serrano, J. A. et al.
Characterization of Minerals, Metals, and Materials 2023. ed. / Mingming Zhang; Zhiwei Peng; Bowen Li; Jiann-Yang Hwang; Sergio Neves Monteiro; Rajiv Soman; Yunus Eren Kalay; Juan P. Escobedo-Diaz; John S. Carpenter; Andrew D. Brown; Shadia Ikhmayies. Springer Science and Business Media Deutschland GmbH, 2023. p. 553-559 (Minerals, Metals and Materials Series).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Structural Characterization of Europium-Doped BaTiO3 Obtained by Solid-State Reaction Synthesis

AU - Hernández-Lara, J. P.

AU - Hernández-Ramírez, A.

AU - Romero-Serrano, J. A.

AU - Pérez-Labra, M.

AU - Barrientos-Hernández, F. R.

AU - Martinez-Lopez, R.

AU - Valenzuela-Carrillo, M. I.

PY - 2023

Y1 - 2023

N2 - Barium Titanate (BaTiO3)-based ceramic materials are widely used in the electroceramic industry. Conventional processing of these materials is primarily in high-temperature solid-state reactions between mixed oxides. To produce a better quality of the initial powder, factors such as the quality of raw materials, homogeneity of the mixture and the nature of the reaction atmosphere must be controlled. In this research, an analysis of BaTiO3-based ceramic products doped with Europium (Eu3+) were carried out, by means of solid-state reaction synthesis. A review of the compositions (x = 0.007 and x = 0.01% by weight Eu3+) was carried out, grinding was carried out for 5 h and the resulting powders were calcined at 900 °C and sintered at 1350 °C. The experimental results by x-ray diffraction showed the tetragonal BaTiO3 phase. Raman spectroscopy analysis shows the phase transition of BaTiO3 ceramics. Scanning electron microscopy results showed randomly round particles.

AB - Barium Titanate (BaTiO3)-based ceramic materials are widely used in the electroceramic industry. Conventional processing of these materials is primarily in high-temperature solid-state reactions between mixed oxides. To produce a better quality of the initial powder, factors such as the quality of raw materials, homogeneity of the mixture and the nature of the reaction atmosphere must be controlled. In this research, an analysis of BaTiO3-based ceramic products doped with Europium (Eu3+) were carried out, by means of solid-state reaction synthesis. A review of the compositions (x = 0.007 and x = 0.01% by weight Eu3+) was carried out, grinding was carried out for 5 h and the resulting powders were calcined at 900 °C and sintered at 1350 °C. The experimental results by x-ray diffraction showed the tetragonal BaTiO3 phase. Raman spectroscopy analysis shows the phase transition of BaTiO3 ceramics. Scanning electron microscopy results showed randomly round particles.

KW - Europium

KW - Raman spectroscopy

KW - Solid state reaction

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U2 - 10.1007/978-3-031-22576-5_56

DO - 10.1007/978-3-031-22576-5_56

M3 - Contribución a la conferencia

AN - SCOPUS:85151128356

SN - 9783031225758

T3 - Minerals, Metals and Materials Series

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BT - Characterization of Minerals, Metals, and Materials 2023

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A2 - Peng, Zhiwei

A2 - Li, Bowen

A2 - Hwang, Jiann-Yang

A2 - Monteiro, Sergio Neves

A2 - Soman, Rajiv

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A2 - Escobedo-Diaz, Juan P.

A2 - Carpenter, John S.

A2 - Brown, Andrew D.

A2 - Ikhmayies, Shadia

PB - Springer Science and Business Media Deutschland GmbH

T2 - Characterization of Minerals, Metals, and Materials Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023

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Hernández-Lara JP, Hernández-Ramírez A , Romero-Serrano JA, Pérez-Labra M, Barrientos-Hernández FR, Martinez-Lopez R et al. Structural Characterization of Europium-Doped BaTiO₃ Obtained by Solid-State Reaction Synthesis. In Zhang M, Peng Z, Li B, Hwang JY, Monteiro SN, Soman R, Kalay YE, Escobedo-Diaz JP, Carpenter JS, Brown AD, Ikhmayies S, editors, Characterization of Minerals, Metals, and Materials 2023. Springer Science and Business Media Deutschland GmbH. 2023. p. 553-559. (Minerals, Metals and Materials Series). doi: 10.1007/978-3-031-22576-5_56