Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye

Vicente Garibay Febles; Dulce Viridiana Melo-Máximo; Isaías Hernández Perez; Raúl Suárez Parra; Julio César Espinoza-Tapia; Ricardo Luna Paz; Lucia Diaz-Barriga Arceo; Jesús Noé Rivera Olvera; Lizbeth Melo-Máximo; Leonardo González-Reyes

doi:10.3390/cryst12081123

Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye

Vicente Garibay Febles, Dulce Viridiana Melo-Máximo, Isaías Hernández Perez, Raúl Suárez Parra, Julio César Espinoza-Tapia, Ricardo Luna Paz, Lucia Diaz-Barriga Arceo, Jesús Noé Rivera Olvera, Lizbeth Melo-Máximo, Leonardo González-Reyes

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2 Scopus citations

Abstract

This study investigates the thermal decomposition of acetyl acetonates of Ni(II) and Fe(III) via a sonochemical process at 20 kHz for 50 min. In the absence of magnetic fields the reactions of Ni(II) and Fe(III) acetyl acetonates under ultrasonic treatment produce Ni(OH)₂ and FeO(OH) nanoparticles coated with carbon. The synthesized materials with different Ni-Fe stoichiometries, Ni90-Fe10, Ni80-Fe20, and Ni50-Fe50 wt%, were subjected to catalytic activity for dye decolorization of Reactive Black 5 (RB5, 100 mg/L) at room temperature using visible radiation. The correlation between the structural and optoelectronic properties and the catalytic performance of the Ni-Fe system with different stoichiometries is reported.

Original language	English
Article number	1123
Journal	Crystals
Volume	12
Issue number	8
DOIs	https://doi.org/10.3390/cryst12081123
State	Published - Aug 2022
Externally published	Yes

Keywords

Ni-Fe
Reactive Black 5
photocatalysis
sonochemistry

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10.3390/cryst12081123

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Garibay Febles, V., Melo-Máximo, D. V., Hernández Perez, I., Suárez Parra, R., Espinoza-Tapia, J. C., Luna Paz, R., Diaz-Barriga Arceo, L., Rivera Olvera, J. N., Melo-Máximo, L., & González-Reyes, L. (2022). Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye. Crystals, 12(8), Article 1123. https://doi.org/10.3390/cryst12081123

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title = "Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye",

abstract = "This study investigates the thermal decomposition of acetyl acetonates of Ni(II) and Fe(III) via a sonochemical process at 20 kHz for 50 min. In the absence of magnetic fields the reactions of Ni(II) and Fe(III) acetyl acetonates under ultrasonic treatment produce Ni(OH)2 and FeO(OH) nanoparticles coated with carbon. The synthesized materials with different Ni-Fe stoichiometries, Ni90-Fe10, Ni80-Fe20, and Ni50-Fe50 wt%, were subjected to catalytic activity for dye decolorization of Reactive Black 5 (RB5, 100 mg/L) at room temperature using visible radiation. The correlation between the structural and optoelectronic properties and the catalytic performance of the Ni-Fe system with different stoichiometries is reported.",

keywords = "Ni-Fe, Reactive Black 5, photocatalysis, sonochemistry",

author = "{Garibay Febles}, Vicente and Melo-M{\'a}ximo, {Dulce Viridiana} and {Hern{\'a}ndez Perez}, Isa{\'i}as and {Su{\'a}rez Parra}, Ra{\'u}l and Espinoza-Tapia, {Julio C{\'e}sar} and {Luna Paz}, Ricardo and {Diaz-Barriga Arceo}, Lucia and {Rivera Olvera}, {Jes{\'u}s No{\'e}} and Lizbeth Melo-M{\'a}ximo and Leonardo Gonz{\'a}lez-Reyes",

note = "Publisher Copyright: {\textcopyright} 2022 by the authors.",

year = "2022",

month = aug,

doi = "10.3390/cryst12081123",

language = "Ingl{\'e}s",

volume = "12",

journal = "Crystals",

issn = "2073-4352",

publisher = "Multidisciplinary Digital Publishing Institute",

number = "8",

}

Garibay Febles, V, Melo-Máximo, DV, Hernández Perez, I, Suárez Parra, R, Espinoza-Tapia, JC, Luna Paz, R, Diaz-Barriga Arceo, L, Rivera Olvera, JN, Melo-Máximo, L & González-Reyes, L 2022, 'Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye', Crystals, vol. 12, no. 8, 1123. https://doi.org/10.3390/cryst12081123

TY - JOUR

T1 - Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye

AU - Garibay Febles, Vicente

AU - Melo-Máximo, Dulce Viridiana

AU - Hernández Perez, Isaías

AU - Suárez Parra, Raúl

AU - Espinoza-Tapia, Julio César

AU - Luna Paz, Ricardo

AU - Diaz-Barriga Arceo, Lucia

AU - Rivera Olvera, Jesús Noé

AU - Melo-Máximo, Lizbeth

AU - González-Reyes, Leonardo

PY - 2022/8

Y1 - 2022/8

N2 - This study investigates the thermal decomposition of acetyl acetonates of Ni(II) and Fe(III) via a sonochemical process at 20 kHz for 50 min. In the absence of magnetic fields the reactions of Ni(II) and Fe(III) acetyl acetonates under ultrasonic treatment produce Ni(OH)2 and FeO(OH) nanoparticles coated with carbon. The synthesized materials with different Ni-Fe stoichiometries, Ni90-Fe10, Ni80-Fe20, and Ni50-Fe50 wt%, were subjected to catalytic activity for dye decolorization of Reactive Black 5 (RB5, 100 mg/L) at room temperature using visible radiation. The correlation between the structural and optoelectronic properties and the catalytic performance of the Ni-Fe system with different stoichiometries is reported.

AB - This study investigates the thermal decomposition of acetyl acetonates of Ni(II) and Fe(III) via a sonochemical process at 20 kHz for 50 min. In the absence of magnetic fields the reactions of Ni(II) and Fe(III) acetyl acetonates under ultrasonic treatment produce Ni(OH)2 and FeO(OH) nanoparticles coated with carbon. The synthesized materials with different Ni-Fe stoichiometries, Ni90-Fe10, Ni80-Fe20, and Ni50-Fe50 wt%, were subjected to catalytic activity for dye decolorization of Reactive Black 5 (RB5, 100 mg/L) at room temperature using visible radiation. The correlation between the structural and optoelectronic properties and the catalytic performance of the Ni-Fe system with different stoichiometries is reported.

KW - Ni-Fe

KW - Reactive Black 5

KW - photocatalysis

KW - sonochemistry

UR - http://www.scopus.com/inward/record.url?scp=85137414041&partnerID=8YFLogxK

U2 - 10.3390/cryst12081123

DO - 10.3390/cryst12081123

M3 - Artículo

AN - SCOPUS:85137414041

SN - 2073-4352

VL - 12

JO - Crystals

JF - Crystals

IS - 8

M1 - 1123

ER -

Sonochemical Synthesis of Nanostructured Ni-Fe-C System and Its Catalytic Activity Based on Decolorization of Reactive Black 5 Dye

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Keywords

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