TY - JOUR
T1 - Microstructure of alumina-matrix composites reinforced with nanometric titanium and titanium carbide dispersions
AU - Refugio-García, Elizabeth
AU - Hernández-Silva, David
AU - Terrés-Rojas, Eduardo
AU - Rodríguez-García, José Amparo
AU - Rocha-Rangel, Enrique
PY - 2012/11
Y1 - 2012/11
N2 - The synthesis of alumina (Al2O3)-composites having different amount of very fine titanium and titanium carbide reinforcement- particles has been explored. Two experimental steps have been set for the synthesis; the first step consisted of the pressureless-sintering of Al 2O3-titanium powders which were thoroughly mixed under high energy ball-milling and through the second step it was induced the formation of titanium carbide during different times at 500 °C by the cementation packing process. SEM and EDS analysis of the microstructures obtained in both sintered and cemented bodies were performed in order to know the effect of the activated carbon used as cementing agent on the titanium for each studied composite. It was observed that a titanium carbide layer growth from the surface into the bulk and reaches different depth as the titanium content in the composites increases. On the other hand, the use of ductile titanium notably enhanced density level and fracture toughness of the composites.
AB - The synthesis of alumina (Al2O3)-composites having different amount of very fine titanium and titanium carbide reinforcement- particles has been explored. Two experimental steps have been set for the synthesis; the first step consisted of the pressureless-sintering of Al 2O3-titanium powders which were thoroughly mixed under high energy ball-milling and through the second step it was induced the formation of titanium carbide during different times at 500 °C by the cementation packing process. SEM and EDS analysis of the microstructures obtained in both sintered and cemented bodies were performed in order to know the effect of the activated carbon used as cementing agent on the titanium for each studied composite. It was observed that a titanium carbide layer growth from the surface into the bulk and reaches different depth as the titanium content in the composites increases. On the other hand, the use of ductile titanium notably enhanced density level and fracture toughness of the composites.
KW - Alumina-composites
KW - Cementation packing process
KW - Metallic-renforcements
UR - http://www.scopus.com/inward/record.url?scp=84870438414&partnerID=8YFLogxK
U2 - 10.1590/S1516-14392012005000110
DO - 10.1590/S1516-14392012005000110
M3 - Artículo
SN - 1516-1439
VL - 15
SP - 898
EP - 902
JO - Materials Research
JF - Materials Research
IS - 6
ER -