TY - JOUR
T1 - Friction and Wear Behavior of Multilayer [Al/AlN]n Coatings Deposited on AISI52100 Steel
AU - Eduardo Alfaro-Pérez, Alfaro-Pérez
AU - Chiñas-Castillo, Fernando
AU - Flores-Ruiz, Francisco J.
AU - Alavez-Ramirez, Rafael
AU - Caballero-Caballero, Magdaleno
AU - Lara-Romero, Javier
N1 - Publisher Copyright:
© 2019, Pleiades Publishing, Ltd.
PY - 2019/5/1
Y1 - 2019/5/1
N2 - Abstract: In this study, a set of multilayer hard nanocrystalline coatings of Al/AlN with 35, 55 and 75 bilayer were prepared by DC magnetron sputtering on AISI 52100 steel specimens at nitrogen fractions of 35 and 65% in the Ar + N2 discharge. X-ray diffraction analysis indicates a polycrystalline structure of AlN + Al and AlN phases for 35% N2 and 65% N2 fraction, respectively. Nanoindentation tests showed hardness values from 11 to 19 GPa and elastic modulus of ~200 GPa almost independent of the bilayer number for both, 35% N2 and 65% N2. Tribological tests evaluated with a CSM pin-on-disk tribometer showed a reduction in the wear rate compared to AISI 52100 steel specimens. Multilayer coatings deposited at 35% N2 fraction presented a lower friction coefficient than those coatings deposited at 65% N2. The origin of such a decrease in the coefficient of friction was associated with the presence of the Al phase in the coatings deposited at 35% N2. The wear mechanism for both 35 and 65% N2 were different. For the first case, the wear is controlled by plastic flow and abrasive wear, while in the second case, is dominated by adhesive wear.
AB - Abstract: In this study, a set of multilayer hard nanocrystalline coatings of Al/AlN with 35, 55 and 75 bilayer were prepared by DC magnetron sputtering on AISI 52100 steel specimens at nitrogen fractions of 35 and 65% in the Ar + N2 discharge. X-ray diffraction analysis indicates a polycrystalline structure of AlN + Al and AlN phases for 35% N2 and 65% N2 fraction, respectively. Nanoindentation tests showed hardness values from 11 to 19 GPa and elastic modulus of ~200 GPa almost independent of the bilayer number for both, 35% N2 and 65% N2. Tribological tests evaluated with a CSM pin-on-disk tribometer showed a reduction in the wear rate compared to AISI 52100 steel specimens. Multilayer coatings deposited at 35% N2 fraction presented a lower friction coefficient than those coatings deposited at 65% N2. The origin of such a decrease in the coefficient of friction was associated with the presence of the Al phase in the coatings deposited at 35% N2. The wear mechanism for both 35 and 65% N2 were different. For the first case, the wear is controlled by plastic flow and abrasive wear, while in the second case, is dominated by adhesive wear.
KW - Al/AlN
KW - multilayer
KW - nanocrystalline
KW - sputtering
KW - tribological
UR - http://www.scopus.com/inward/record.url?scp=85067834430&partnerID=8YFLogxK
U2 - 10.1134/S207020511903002X
DO - 10.1134/S207020511903002X
M3 - Artículo
AN - SCOPUS:85067834430
SN - 2070-2051
VL - 55
SP - 527
EP - 534
JO - Protection of Metals and Physical Chemistry of Surfaces
JF - Protection of Metals and Physical Chemistry of Surfaces
IS - 3
ER -