TY - JOUR
T1 - Cinética de engrosamiento de precipitados coherentes en la aleación Fe-10 % Ni-15 % Al
AU - Cayetano-Castro, N.
AU - Dorantes-Rosales, H. J.
AU - López-Hirata, V. M.
AU - Cruz-Rivera, J. J.
AU - Moreno-Palmerin, J.
AU - González-Velázquez, J. L.
PY - 2008
Y1 - 2008
N2 - The coarsening kinetics and the morphology evolution of the coherent β' (Fe, Ni)Al precipitates embedded in a ferritic matrix were studied in the aged Fe-10 % Ni-15 % Al alloy. Samples were solution treated at 1,100°C for 24 h and subsequently aged at 750, 850 and 920°C for different times. XRD, SEM and TEM results showed the following decomposition reaction after aging treatment, αsss →α+β. Intragranular particles distribution changes from a random to an aligned on the elastically soft 〈100〉 crystallographic directions of the matrix. Additionally, the morphological evolution of the precipitates was as follows: spheres → cuboids → parallelepipeds → plates. The variation of the cube of mean radius of particles, r3, and the particle density as a function of time followed a linear relationship, as predicted by the Lifshitz, Slyosov and Wagner (LSW) theory for diffusion-controlled coarsening. The rate constant (K) increased with the aging temperature. The activation energy for coarsening process was determined to be about of 220 kJ/mol.
AB - The coarsening kinetics and the morphology evolution of the coherent β' (Fe, Ni)Al precipitates embedded in a ferritic matrix were studied in the aged Fe-10 % Ni-15 % Al alloy. Samples were solution treated at 1,100°C for 24 h and subsequently aged at 750, 850 and 920°C for different times. XRD, SEM and TEM results showed the following decomposition reaction after aging treatment, αsss →α+β. Intragranular particles distribution changes from a random to an aligned on the elastically soft 〈100〉 crystallographic directions of the matrix. Additionally, the morphological evolution of the precipitates was as follows: spheres → cuboids → parallelepipeds → plates. The variation of the cube of mean radius of particles, r3, and the particle density as a function of time followed a linear relationship, as predicted by the Lifshitz, Slyosov and Wagner (LSW) theory for diffusion-controlled coarsening. The rate constant (K) increased with the aging temperature. The activation energy for coarsening process was determined to be about of 220 kJ/mol.
KW - Aging
KW - Coarsening
KW - Coherent precipitates
KW - Fe-ni-al alloy
KW - Phase transformations
UR - http://www.scopus.com/inward/record.url?scp=47049100151&partnerID=8YFLogxK
U2 - 10.3989/revmetalm.2008.v44.i2.104
DO - 10.3989/revmetalm.2008.v44.i2.104
M3 - Artículo
SN - 0034-8570
VL - 44
SP - 162
EP - 169
JO - Revista de Metalurgia (Madrid)
JF - Revista de Metalurgia (Madrid)
IS - 2
ER -