TY - JOUR
T1 - Chitosan-coated magnetic nanoparticles with low chitosan content prepared in one-step
AU - Osuna, Yolanda
AU - Gregorio-Jauregui, Karla M.
AU - Gaona-Lozano, J. Gerardo
AU - De La Garza-Rodríguez, Iliana M.
AU - Ilyna, Anna
AU - Barriga-Castro, Enrique Díaz
AU - Saade, Hened
AU - López, Raúl G.
PY - 2012
Y1 - 2012
N2 - Chitosan-coated magnetic nanoparticles (CMNP) were obtained at 50°C in a one-step method comprising coprecipitation in the presence of low chitosan content. CMNP showed high magnetization and superparamagnetism. They were composed of a core of 9.5 nm in average diameter and a very thin chitosan layer in accordance with electron microscopy measurements. The results from Fourier transform infrared spectrometry demonstrated that CMNP were obtained and those from thermogravimetric analysis allowed to determine that they were composed of 95 wt of magnetic nanoparticles and 5 wt of chitosan. 67 efficacy in the Pb +2 removal test indicated that only 60 of amino groups on CMNP surface bound to Pb, probably due to some degree of nanoparticle flocculation during the redispersion. The very low weight ratio chitosan to magnetic nanoparticles obtained in this study, 0.053, and the high yield of the precipitation reactions (≈97%) are noticeable.
AB - Chitosan-coated magnetic nanoparticles (CMNP) were obtained at 50°C in a one-step method comprising coprecipitation in the presence of low chitosan content. CMNP showed high magnetization and superparamagnetism. They were composed of a core of 9.5 nm in average diameter and a very thin chitosan layer in accordance with electron microscopy measurements. The results from Fourier transform infrared spectrometry demonstrated that CMNP were obtained and those from thermogravimetric analysis allowed to determine that they were composed of 95 wt of magnetic nanoparticles and 5 wt of chitosan. 67 efficacy in the Pb +2 removal test indicated that only 60 of amino groups on CMNP surface bound to Pb, probably due to some degree of nanoparticle flocculation during the redispersion. The very low weight ratio chitosan to magnetic nanoparticles obtained in this study, 0.053, and the high yield of the precipitation reactions (≈97%) are noticeable.
UR - http://www.scopus.com/inward/record.url?scp=84868691669&partnerID=8YFLogxK
U2 - 10.1155/2012/327562
DO - 10.1155/2012/327562
M3 - Artículo
AN - SCOPUS:84868691669
SN - 1687-4110
VL - 2012
JO - Journal of Nanomaterials
JF - Journal of Nanomaterials
M1 - 327562
ER -