TY - JOUR
T1 - Study of microcracks morphology produced by Vickers indentation on AISI 1045 borided steels
AU - Campos, I.
AU - Ramírez, G.
AU - VillaVelázquez, C.
AU - Figueroa, U.
AU - Rodríguez, G.
N1 - Funding Information:
This work has been supported by the research grant 20070130 of Instituto Politécnico Nacional at Mexico. The authors would like to thank Prof. Alexander Balankin for useful discussions.
PY - 2008/2/25
Y1 - 2008/2/25
N2 - In this work, we analyzed the roughness morphology of indentation microcracks produced by the Vickers microindentation in the iron boride Fe2B. Using the paste boriding process, the boride layers were formed at the surface of AISI 1045 steels. The diffusion processes were carried out with 5 mm of boron paste thickness over the substrate surface at three different temperatures (1193, 1223 and 1273 K) with two different time exposures. The indentations in each Fe2B layer were made using a constant load of 200 g at four different distances from the surface. The fracture behavior of the Fe2B borided phase is found to be brittle in nature. The profiles of microcracks formed at the corners of the indentations were obtained using the scanning electronic microscopy and were analyzed within the framework of fractal geometry. We found that all indentation microcracks display a self-affine invariance characterized by the same roughness (Hurst) exponent H = 0.8 ± 0.1. The effect of the self-affine roughness of indentation microcracks on the measured fracture toughness is discussed within the framework of the mechanics of self-affine cracks. It is pointed out that the arrest of indentation microcracks is controlled by the fractal fracture toughness, which for the Fe2B borided phase is found to be Kfc = 0.42 ± 0.02 MPa m0.75 at all distances from the surface.
AB - In this work, we analyzed the roughness morphology of indentation microcracks produced by the Vickers microindentation in the iron boride Fe2B. Using the paste boriding process, the boride layers were formed at the surface of AISI 1045 steels. The diffusion processes were carried out with 5 mm of boron paste thickness over the substrate surface at three different temperatures (1193, 1223 and 1273 K) with two different time exposures. The indentations in each Fe2B layer were made using a constant load of 200 g at four different distances from the surface. The fracture behavior of the Fe2B borided phase is found to be brittle in nature. The profiles of microcracks formed at the corners of the indentations were obtained using the scanning electronic microscopy and were analyzed within the framework of fractal geometry. We found that all indentation microcracks display a self-affine invariance characterized by the same roughness (Hurst) exponent H = 0.8 ± 0.1. The effect of the self-affine roughness of indentation microcracks on the measured fracture toughness is discussed within the framework of the mechanics of self-affine cracks. It is pointed out that the arrest of indentation microcracks is controlled by the fractal fracture toughness, which for the Fe2B borided phase is found to be Kfc = 0.42 ± 0.02 MPa m0.75 at all distances from the surface.
KW - Boride layers
KW - Fractal fracture toughness
KW - Paste boriding
KW - Roughness morphology
KW - Self-affine cracks
UR - http://www.scopus.com/inward/record.url?scp=38849094635&partnerID=8YFLogxK
U2 - 10.1016/j.msea.2007.04.052
DO - 10.1016/j.msea.2007.04.052
M3 - Artículo
SN - 0921-5093
VL - 475
SP - 285
EP - 292
JO - Materials Science and Engineering A
JF - Materials Science and Engineering A
IS - 1-2
ER -