Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si 3N4 nanocomposite coatings deposited by sputtering on AISI 316L

J. García; C. E. Canto; M. Flores; E. Andrade; E. Rodríguez; O. Jiménez; C. Solis; O. G. De Lucio; M. F. Rocha

doi:10.1016/j.nimb.2013.12.041

Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si ₃N₄ nanocomposite coatings deposited by sputtering on AISI 316L

J. García, C. E. Canto, M. Flores, E. Andrade, E. Rodríguez, O. Jiménez, C. Solis, O. G. De Lucio, M. F. Rocha

Escuela Superior de Ingeniería Mecánica y Eléctrica (ESIME), Unidad Zacatenco

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Resumen

In this work, nanocomposite coatings of nc-TiN/a-Si₃N ₄, were deposited on AISI 316L stainless steel substrate by a DC and RF reactive magnetron co-sputtering technique using an Ar-N₂ plasma. The structure of the coatings was characterized by means of XRD (X-ray Diffraction). The substrate and coating corrosion resistance were evaluated by potentiodynamic polarization using a Ringer solution as electrolyte. Corrosion tests were conducted with the purpose to evaluate the potential of this coating to be used on biomedical alloys. IBA (Ion Beam Analysis) techniques were applied to measure the elemental composition profiles of the films and, XPS (X-ray Photoelectron Spectroscopy) were used as a complementary technique to obtain information about the compounds present in the films. The nanocomposite coatings of nc-TiN/a-Si₃N₄ show crystalline (TiN) and amorphous (Si₃N₄) phases which confer a better protection against the corrosion effects compared with that of the AISI 316L.

Idioma original	Inglés
Páginas (desde-hasta)	130-133
Número de páginas	4
Publicación	Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms
Volumen	331
DOI	https://doi.org/10.1016/j.nimb.2013.12.041
Estado	Publicada - 15 jul. 2014

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García, J., Canto, C. E., Flores, M., Andrade, E., Rodríguez, E., Jiménez, O., Solis, C., De Lucio, O. G., & Rocha, M. F. (2014). Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si ₃N₄ nanocomposite coatings deposited by sputtering on AISI 316L. Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, 331, 130-133. https://doi.org/10.1016/j.nimb.2013.12.041

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title = "Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si 3N4 nanocomposite coatings deposited by sputtering on AISI 316L",

abstract = "In this work, nanocomposite coatings of nc-TiN/a-Si3N 4, were deposited on AISI 316L stainless steel substrate by a DC and RF reactive magnetron co-sputtering technique using an Ar-N2 plasma. The structure of the coatings was characterized by means of XRD (X-ray Diffraction). The substrate and coating corrosion resistance were evaluated by potentiodynamic polarization using a Ringer solution as electrolyte. Corrosion tests were conducted with the purpose to evaluate the potential of this coating to be used on biomedical alloys. IBA (Ion Beam Analysis) techniques were applied to measure the elemental composition profiles of the films and, XPS (X-ray Photoelectron Spectroscopy) were used as a complementary technique to obtain information about the compounds present in the films. The nanocomposite coatings of nc-TiN/a-Si3N4 show crystalline (TiN) and amorphous (Si3N4) phases which confer a better protection against the corrosion effects compared with that of the AISI 316L.",

keywords = "Corrosion, IBA, Nanocomposite, TiN",

author = "J. Garc{\'i}a and Canto, {C. E.} and M. Flores and E. Andrade and E. Rodr{\'i}guez and O. Jim{\'e}nez and C. Solis and {De Lucio}, {O. G.} and Rocha, {M. F.}",

note = "Funding Information: The authors acknowledge the work and help of Fis. Arcadio Huerta, M. en C. Eustacio P{\'e}rez Zavala for technical assistance. The authors are also in debt to Lazaro Huerta for the XPS measurements. This work has been partially supported by CONACYT, under the Project number 49172 and by the UNAM DGAPA project IN103312. We would like to thank CINVESTAV in Queretaro and UNAM for their support, providing access to their testing equipment and facilities.",

year = "2014",

month = jul,

day = "15",

doi = "10.1016/j.nimb.2013.12.041",

language = "Ingl{\'e}s",

volume = "331",

pages = "130--133",

journal = "Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms",

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García, J, Canto, CE, Flores, M, Andrade, E, Rodríguez, E, Jiménez, O, Solis, C, De Lucio, OG & Rocha, MF 2014, 'Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si ₃N₄ nanocomposite coatings deposited by sputtering on AISI 316L', Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, vol. 331, pp. 130-133. https://doi.org/10.1016/j.nimb.2013.12.041

Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si ₃N₄ nanocomposite coatings deposited by sputtering on AISI 316L. / García, J.; Canto, C. E.; Flores, M. et al.
En: Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, Vol. 331, 15.07.2014, p. 130-133.

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

TY - JOUR

T1 - Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si 3N4 nanocomposite coatings deposited by sputtering on AISI 316L

AU - García, J.

AU - Canto, C. E.

AU - Flores, M.

AU - Andrade, E.

AU - Rodríguez, E.

AU - Jiménez, O.

AU - Solis, C.

AU - De Lucio, O. G.

AU - Rocha, M. F.

N1 - Funding Information: The authors acknowledge the work and help of Fis. Arcadio Huerta, M. en C. Eustacio Pérez Zavala for technical assistance. The authors are also in debt to Lazaro Huerta for the XPS measurements. This work has been partially supported by CONACYT, under the Project number 49172 and by the UNAM DGAPA project IN103312. We would like to thank CINVESTAV in Queretaro and UNAM for their support, providing access to their testing equipment and facilities.

PY - 2014/7/15

Y1 - 2014/7/15

N2 - In this work, nanocomposite coatings of nc-TiN/a-Si3N 4, were deposited on AISI 316L stainless steel substrate by a DC and RF reactive magnetron co-sputtering technique using an Ar-N2 plasma. The structure of the coatings was characterized by means of XRD (X-ray Diffraction). The substrate and coating corrosion resistance were evaluated by potentiodynamic polarization using a Ringer solution as electrolyte. Corrosion tests were conducted with the purpose to evaluate the potential of this coating to be used on biomedical alloys. IBA (Ion Beam Analysis) techniques were applied to measure the elemental composition profiles of the films and, XPS (X-ray Photoelectron Spectroscopy) were used as a complementary technique to obtain information about the compounds present in the films. The nanocomposite coatings of nc-TiN/a-Si3N4 show crystalline (TiN) and amorphous (Si3N4) phases which confer a better protection against the corrosion effects compared with that of the AISI 316L.

AB - In this work, nanocomposite coatings of nc-TiN/a-Si3N 4, were deposited on AISI 316L stainless steel substrate by a DC and RF reactive magnetron co-sputtering technique using an Ar-N2 plasma. The structure of the coatings was characterized by means of XRD (X-ray Diffraction). The substrate and coating corrosion resistance were evaluated by potentiodynamic polarization using a Ringer solution as electrolyte. Corrosion tests were conducted with the purpose to evaluate the potential of this coating to be used on biomedical alloys. IBA (Ion Beam Analysis) techniques were applied to measure the elemental composition profiles of the films and, XPS (X-ray Photoelectron Spectroscopy) were used as a complementary technique to obtain information about the compounds present in the films. The nanocomposite coatings of nc-TiN/a-Si3N4 show crystalline (TiN) and amorphous (Si3N4) phases which confer a better protection against the corrosion effects compared with that of the AISI 316L.

KW - Corrosion

KW - IBA

KW - Nanocomposite

KW - TiN

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U2 - 10.1016/j.nimb.2013.12.041

DO - 10.1016/j.nimb.2013.12.041

M3 - Artículo

SN - 0168-583X

VL - 331

SP - 130

EP - 133

JO - Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms

JF - Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms

ER -

García J, Canto CE, Flores M, Andrade E, Rodríguez E, Jiménez O et al. Ion Beam Analysis, structure and corrosion studies of nc-TiN/a-Si ₃N₄ nanocomposite coatings deposited by sputtering on AISI 316L. Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms. 2014 jul. 15;331:130-133. doi: 10.1016/j.nimb.2013.12.041