TY - JOUR
T1 - Experimental protocol for HOR and ORR in alkaline electrochemical measurements
AU - Campos-Roldán, C. A.
AU - González-Huerta, R. G.
AU - Alonso-Vante, N.
N1 - Publisher Copyright:
© The Author(s) 2018. Published by ECS.
PY - 2018
Y1 - 2018
N2 - This work revises the essentials of electrocatalytic electrochemical measurement done in alkaline electrolytes. The hydrogen oxidation reaction (HOR) and the oxygen reduction reaction (ORR) were considered as a baseline to understand some key critical factors in a half-cell system. The material considered herein was essentially the carbon supported platinum nanoparticles as benchmark material. The main electrochemical techniques considered were cyclic voltammetry (CV) and the rotating disk electrode (RDE). The critical factors considered were the electrochemical cell vessel, reference electrode, nature of the cation in the alkaline electrolyte, and ohmic drop correction.
AB - This work revises the essentials of electrocatalytic electrochemical measurement done in alkaline electrolytes. The hydrogen oxidation reaction (HOR) and the oxygen reduction reaction (ORR) were considered as a baseline to understand some key critical factors in a half-cell system. The material considered herein was essentially the carbon supported platinum nanoparticles as benchmark material. The main electrochemical techniques considered were cyclic voltammetry (CV) and the rotating disk electrode (RDE). The critical factors considered were the electrochemical cell vessel, reference electrode, nature of the cation in the alkaline electrolyte, and ohmic drop correction.
UR - http://www.scopus.com/inward/record.url?scp=85050383428&partnerID=8YFLogxK
U2 - 10.1149/2.0011815jes
DO - 10.1149/2.0011815jes
M3 - Artículo
AN - SCOPUS:85050383428
SN - 0013-4651
VL - 165
SP - J3001-J3007
JO - Journal of the Electrochemical Society
JF - Journal of the Electrochemical Society
IS - 15
ER -