Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi1.6Pb0.4Sr2Ca2Cu3Oy superconductor

M. Romero-Sánchez; T. Sánchez-Mera; J. Santos-Cruz; C. E. Pérez-García; M. de la L. Olvera; C. R. Santillán-Rodríguez; J. Matutes-Aquino; G. Contreras-Puente; F. de Moure-Flores

doi:10.1016/j.ceramint.2022.02.149

Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi_1.6Pb_0.4Sr₂Ca₂Cu₃O_y superconductor

M. Romero-Sánchez, T. Sánchez-Mera, J. Santos-Cruz, C. E. Pérez-García, M. de la L. Olvera, C. R. Santillán-Rodríguez, J. Matutes-Aquino, G. Contreras-Puente, F. de Moure-Flores

Escuela Superior de Física y Matemáticas (ESFM)

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

6 Citas (Scopus)

Resumen

Bi_1.6Pb_0.4Sb_0.06Sr₂Ca₂Cu₃O_y superconductors were processed by the solid-state reaction at 860 °C, varying the sintering time from 100 to 160 h. The structural characterization was carried out by X-ray diffraction and Raman spectroscopy, which showed that Bi_1.6Pb_0.4Sb_0.06Sr₂Ca₂Cu₃O_y samples have a mixture of interest B-2212 and Bi-2223 phases. The sintering time strongly influences structural, morphological and electrical properties; the sample sintered by 130 h presents a volume fraction of 62% for the Bi-2223 phase, large grains (between 5 and 20 μm) and a critical temperature of 107 K.

Idioma original	Inglés
Páginas (desde-hasta)	16049-16053
Número de páginas	5
Publicación	Ceramics International
Volumen	48
N.º	11
DOI	https://doi.org/10.1016/j.ceramint.2022.02.149
Estado	Publicada - 1 jun. 2022

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Romero-Sánchez, M., Sánchez-Mera, T., Santos-Cruz, J., Pérez-García, C. E., Olvera, M. D. L. L., Santillán-Rodríguez, C. R., Matutes-Aquino, J., Contreras-Puente, G., & de Moure-Flores, F. (2022). Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi_1.6Pb_0.4Sr₂Ca₂Cu₃O_y superconductor. Ceramics International, 48(11), 16049-16053. https://doi.org/10.1016/j.ceramint.2022.02.149

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title = "Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi1.6Pb0.4Sr2Ca2Cu3Oy superconductor",

abstract = "Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy superconductors were processed by the solid-state reaction at 860 °C, varying the sintering time from 100 to 160 h. The structural characterization was carried out by X-ray diffraction and Raman spectroscopy, which showed that Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy samples have a mixture of interest B-2212 and Bi-2223 phases. The sintering time strongly influences structural, morphological and electrical properties; the sample sintered by 130 h presents a volume fraction of 62% for the Bi-2223 phase, large grains (between 5 and 20 μm) and a critical temperature of 107 K.",

keywords = "BSCCO superconductor, Sintering time, Solid-state reaction",

author = "M. Romero-S{\'a}nchez and T. S{\'a}nchez-Mera and J. Santos-Cruz and P{\'e}rez-Garc{\'i}a, {C. E.} and Olvera, {M. de la L.} and Santill{\'a}n-Rodr{\'i}guez, {C. R.} and J. Matutes-Aquino and G. Contreras-Puente and {de Moure-Flores}, F.",

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Romero-Sánchez, M, Sánchez-Mera, T, Santos-Cruz, J, Pérez-García, CE, Olvera, MDLL, Santillán-Rodríguez, CR, Matutes-Aquino, J, Contreras-Puente, G & de Moure-Flores, F 2022, 'Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi_1.6Pb_0.4Sr₂Ca₂Cu₃O_y superconductor', Ceramics International, vol. 48, n.º 11, pp. 16049-16053. https://doi.org/10.1016/j.ceramint.2022.02.149

TY - JOUR

T1 - Effect of sintering time on structural, morphological and electrical properties of Sb-doped Bi1.6Pb0.4Sr2Ca2Cu3Oy superconductor

AU - Romero-Sánchez, M.

AU - Sánchez-Mera, T.

AU - Santos-Cruz, J.

AU - Pérez-García, C. E.

AU - Olvera, M. de la L.

AU - Santillán-Rodríguez, C. R.

AU - Matutes-Aquino, J.

AU - Contreras-Puente, G.

AU - de Moure-Flores, F.

PY - 2022/6/1

Y1 - 2022/6/1

N2 - Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy superconductors were processed by the solid-state reaction at 860 °C, varying the sintering time from 100 to 160 h. The structural characterization was carried out by X-ray diffraction and Raman spectroscopy, which showed that Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy samples have a mixture of interest B-2212 and Bi-2223 phases. The sintering time strongly influences structural, morphological and electrical properties; the sample sintered by 130 h presents a volume fraction of 62% for the Bi-2223 phase, large grains (between 5 and 20 μm) and a critical temperature of 107 K.

AB - Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy superconductors were processed by the solid-state reaction at 860 °C, varying the sintering time from 100 to 160 h. The structural characterization was carried out by X-ray diffraction and Raman spectroscopy, which showed that Bi1.6Pb0.4Sb0.06Sr2Ca2Cu3Oy samples have a mixture of interest B-2212 and Bi-2223 phases. The sintering time strongly influences structural, morphological and electrical properties; the sample sintered by 130 h presents a volume fraction of 62% for the Bi-2223 phase, large grains (between 5 and 20 μm) and a critical temperature of 107 K.

KW - BSCCO superconductor

KW - Sintering time

KW - Solid-state reaction

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M3 - Artículo

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JO - Ceramics International

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