Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films

A. García-Murillo, C. Le Luyer, C. Pedrini, J. Mugnier

Research output: Contribution to conferencePaper

32 Citations (Scopus)

Abstract

Lutetium oxide films have been prepared by the sol-gel method and the dip-coating technique. Transparent and crack free coatings are obtained. Differential Thermal Analysis and Infrared spectroscopy were conducted on the dried sol-gel solution in order to determine the structure dependence of the material with temperature. The film microstructure was studied by Raman microscopy and X-ray diffraction. The crystallization of the lutetium oxide phase occurs at 600°C. Opto-geometrical parameters were determined depending on the annealing temperature. After heat treatment at 1000°C, very dense lutetium oxide films are obtained exhibiting a refractive index around 1.8 at 543.5 nm and a thickness of 410 nm. © 2001 Elsevier Science B.V.
Original languageAmerican English
Pages74-77
Number of pages66
DOIs
StatePublished - 12 Jul 2001
Externally publishedYes
EventJournal of Alloys and Compounds -
Duration: 28 Apr 2004 → …

Conference

ConferenceJournal of Alloys and Compounds
Period28/04/04 → …

Fingerprint

Lutetium
Polymethyl Methacrylate
Oxides
Gels
Differential Thermal Analysis
Refractometry
Temperature
Crystallization
X-Ray Diffraction
Microscopy
Spectrum Analysis
Hot Temperature

Cite this

García-Murillo, A., Le Luyer, C., Pedrini, C., & Mugnier, J. (2001). Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films. 74-77. Paper presented at Journal of Alloys and Compounds, . https://doi.org/10.1016/S0925-8388(01)00989-6
García-Murillo, A. ; Le Luyer, C. ; Pedrini, C. ; Mugnier, J. / Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films. Paper presented at Journal of Alloys and Compounds, .66 p.
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García-Murillo, A, Le Luyer, C, Pedrini, C & Mugnier, J 2001, 'Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films', Paper presented at Journal of Alloys and Compounds, 28/04/04 pp. 74-77. https://doi.org/10.1016/S0925-8388(01)00989-6

Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films. / García-Murillo, A.; Le Luyer, C.; Pedrini, C.; Mugnier, J.

2001. 74-77 Paper presented at Journal of Alloys and Compounds, .

Research output: Contribution to conferencePaper

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AB - Lutetium oxide films have been prepared by the sol-gel method and the dip-coating technique. Transparent and crack free coatings are obtained. Differential Thermal Analysis and Infrared spectroscopy were conducted on the dried sol-gel solution in order to determine the structure dependence of the material with temperature. The film microstructure was studied by Raman microscopy and X-ray diffraction. The crystallization of the lutetium oxide phase occurs at 600°C. Opto-geometrical parameters were determined depending on the annealing temperature. After heat treatment at 1000°C, very dense lutetium oxide films are obtained exhibiting a refractive index around 1.8 at 543.5 nm and a thickness of 410 nm. © 2001 Elsevier Science B.V.

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García-Murillo A, Le Luyer C, Pedrini C, Mugnier J. Synthesis and properties of Lu <inf>2</inf> O <inf>3</inf> sol-gel films. 2001. Paper presented at Journal of Alloys and Compounds, . https://doi.org/10.1016/S0925-8388(01)00989-6