TY - JOUR
T1 - Preparation and characterization of TiN powder by reactive milling in air
AU - Orea-Lara, Joaquina
AU - Balmori-Ramírez, Heberto
AU - de anda-Salazar, F. J.
AU - Yee-Madeira, H.
PY - 2012
Y1 - 2012
N2 - TiN powder was obtained by the reactive milling of a titanium powder in an air atmosphere, utilizing an attrition mill. Characterization of the powders was carried out by means of chemical analysis, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The reaction took place over a period of 96 hours in the attrition mill. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in the mill, with a lattice parameter of 4.38 Å. The morphology of the obtained powders was nodular, having particle sizes within the nanometric size range.
AB - TiN powder was obtained by the reactive milling of a titanium powder in an air atmosphere, utilizing an attrition mill. Characterization of the powders was carried out by means of chemical analysis, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The reaction took place over a period of 96 hours in the attrition mill. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in the mill, with a lattice parameter of 4.38 Å. The morphology of the obtained powders was nodular, having particle sizes within the nanometric size range.
KW - Attrition
KW - Mill
KW - Milling
KW - Powders
KW - TiN
UR - http://www.scopus.com/inward/record.url?scp=84857928528&partnerID=8YFLogxK
M3 - Artículo
SN - 1229-9162
VL - 13
SP - 86
EP - 88
JO - Journal of Ceramic Processing Research
JF - Journal of Ceramic Processing Research
IS - 1
ER -